Thursday, March 3, 2011

Acid Analysis by Titration Determination of Molecular Weight

Table 1. Data from standardization of NaOH titrant with KHP.

Trial
Mass KHP (g)
Initial Burette Volume (mL)
Finial Burette Volume (mL)
NaOH Concentration (M)
1
0.1133
0.23
20.15
0.02785
2
0.1148
20.15
40.21
0.02802
3
0.1118
20.97
40.38
0.02820
4
0.1104
1.48
20.97
0.02774
The average NaOH concentration was calculated to be 0.02795 M with a standard deviation of 0.00020.
Table 2. Data from molar mass determination of unknown number 519A.

Trial
Mass KHP (g)
Initial Burette Volume (mL)
Finial Burette Volume (mL)
Molar Mass (g/L)
1
0.2175
0.48
18.70
426.7
2
0.2037
18.70
35.31
438.7
3
0.1982
0.28
16.63
433.7
The average molar mass the unknown was determined to be 433.0 g/L with a standard deviation of 6.1.

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